Accession Number : AD0702873

Title :   AN IMPROVED SYNTHESIS OF 1,6-DICARBACLOSODECABORANE(10).

Descriptive Note : Technical rept.,

Corporate Author : CALIFORNIA UNIV LOS ANGELES DEPT OF CHEMISTRY

Personal Author(s) : Garrett,Philip M. ; Ditta,Gary S. ; Hawthorne,M. F.

Report Date : 04 MAR 1970

Pagination or Media Count : 12

Abstract : Hydroboration of a diethyl ether solution of NaB7C2H13/B7C2H13 yields 1,6-B8C2H10 in 74% yield. Recovery of the unreacted B7C2H13 raises the yield to 82%. The C-monomethyl, C,C'-dimethyl, and C-monophenyl derivatives of 1,6-B8C2H10 can be prepared in somewhat higher yields. (Author)

Descriptors :   (*ORGANOBORANES, SYNTHESIS(CHEMISTRY)), (*BORANES, SYNTHESIS(CHEMISTRY)), DIBORANES

Subject Categories : Inorganic Chemistry
      Organic Chemistry

Distribution Statement : APPROVED FOR PUBLIC RELEASE