Accession Number : AD0709795

Title :   PREPARATION OF IODOBENZENE-D5 AND DIPHENYLACETYLENE-D5,

Corporate Author : NATIONAL RESEARCH COUNCIL OF CANADA HALIFAX (NOVA SCOTIA) ATLANTIC REGIONAL LAB

Personal Author(s) : Safe,S.

Report Date : 25 NOV 1969

Pagination or Media Count : 2

Abstract : Iodobenzene-d5 was prepared from readily available benzene-d6. Benzene-d6 was monoiodinated by treatment with either iodic acid, iodine, acetic acid-d4 deuterium oxide and sulfuric acid-d2 to give iodobenzene-d5 in 60-80% yield. (Author)

Descriptors :   (*HALOGENATED HYDROCARBONS, SYNTHESIS(CHEMISTRY)), (*ALKYNES, SYNTHESIS(CHEMISTRY)), IODINE COMPOUNDS, AROMATIC COMPOUNDS, DEUTERIUM COMPOUNDS, CANADA

Subject Categories : Organic Chemistry

Distribution Statement : APPROVED FOR PUBLIC RELEASE