Accession Number : AD0721655

Title :   Synthesis of 12-Hydroxystearic Acid Esters of Tris(1-(2-Methyl) Aziridinyl) Phosphine Oxide.

Descriptive Note : Technical rept.,

Corporate Author : ARMY MISSILE COMMAND REDSTONE ARSENAL ALA PROPULSION DIRECTORATE

Personal Author(s) : Morgan,Donald A.

Report Date : 16 FEB 1971

Pagination or Media Count : 22

Abstract : The report contains the results of an investigation on the synthesis of esters of 12-hydroxystearic acid and tris (1-(2-methyl) aziridinyl) phosphine oxide with low content of free 12-hydroxystearic acid. Favorable conditions of synthesis were found to be not over 100C, not less than 3 hours reaction time, presence of some water, and absence of heavy metals. Products were tentatively identified as the mono- and di-acid esters of the monomer, dimer, and trimer. (Author)

Descriptors :   (*PHOSPHINE OXIDES, CHEMICAL REACTIONS), (*SURFACE ACTIVE SUBSTANCES, SYNTHESIS(CHEMISTRY)), (*STEARATES, SYNTHESIS(CHEMISTRY)), ESTERS, NITROGEN HETEROCYCLIC COMPOUNDS, CHROMATOGRAPHIC ANALYSIS, SOLID ROCKET PROPELLANTS

Subject Categories : Organic Chemistry

Distribution Statement : APPROVED FOR PUBLIC RELEASE