Accession Number : ADA317892

Title :   Facile Preparation of Nanocrystalline Gallium Antimonide.

Descriptive Note : Technical rept.,

Corporate Author : DUKE UNIV DURHAM NC DEPT OF CHEMISTRY

Personal Author(s) : Baldwin, R. A. ; Foos, E. E. ; Wells, R. L.

PDF Url : ADA317892

Report Date : 30 OCT 1996

Pagination or Media Count : 11

Abstract : The 1:1 reaction of GaCl3 with Sb(SiMe3)3 in pentane solution affords an intermediate material which, upon thermolysis, yields nanocrystalline GaSb with an approximate average particle size of 12 nm. The product was characterized through powder X-ray diffraction, elemental analysis, and HRTEM.

Descriptors :   *CRYSTALS, *GALLIUM ANTIMONIDES, MATERIALS, POWDERS, X RAY DIFFRACTION, HIGH RESOLUTION, ELECTRON MICROSCOPY, SOLUTIONS(GENERAL), SILICON, CHEMICAL REACTIONS, CHLORIDES, CHEMICAL ANALYSIS, CHEMICAL ELEMENTS, PENTANES.

Subject Categories : Inorganic Chemistry
      Physical Chemistry
      Crystallography

Distribution Statement : APPROVED FOR PUBLIC RELEASE