Accession Number : ADA322586
Title : The Spectrochemical Assay of Uranium 235 Using Photomultiplier Tubes,
Corporate Author : UNION CARBIDE NUCLEAR CO OAK RIDGE TN
Personal Author(s) : Lee, T. ; Rogers, Lewis H.
PDF Url : ADA322586
Report Date : 31 OCT 1951
Pagination or Media Count : 28
Abstract : A Jarrell-Ash 21 foot grating spectrograph was adapted to direct reading by replacing the photographic plateholder with exit slits and photomultiplier tubes. Using a hollow cathode discharge tube for excitation of the sample and the isotopic shift effect, uranium 235 was determined in several samples by comparison with a single standard. The uranium 235 content of the samples and standards was known from mass spectrometer measurements to within 0.5% of the amount present at the 95% confidence level. For a determination consisting of 10 measurements, the precision obtained was from plus or minus 1.2 to 1.8% of the amount present over a concentration range of from 8% to 11.9% uranium 235.
Descriptors : *MASS SPECTROMETERS, *URANIUM, *ISOTOPE SEPARATION, EXCITATION, GRATINGS(SPECTRA), PHOTOMULTIPLIER TUBES, SPECTRUM ANALYSIS, ASSAYING, SPECTROGRAPHS, ISOTOPE EFFECT, CATHODES(ELECTRON TUBES), DISCHARGE TUBES.
Subject Categories : Radiation and Nuclear Chemistry
Distribution Statement : APPROVED FOR PUBLIC RELEASE