Accession Number : ADD012488

Title :   Technique for the Growth of Compositionally Ungraded Single Crystals of Solid Solutions.

Descriptive Note : Patent,

Corporate Author : DEPARTMENT OF THE AIR FORCE WASHINGTON DC

Personal Author(s) : Marshall,Robert C ; Kennedy,John K ; Sahagian,Charles S

Report Date : 29 Jul 1986

Pagination or Media Count : 7

Abstract : This invention describes a modified method of growing high purity, compositionally ungraded, single crystals of multicomponent solid solutions by the Czochralski, Kyropoulos, Bridgman or other related melt growth technqiue. In the method of this invention, the container or crucible used to contain the multicomponent crystal growing melt is fabricated from the higher melting point component of the multicompenent melt while lower melting point components are positioned within the crucible. The temperature of the crucible is then raised beyond the melting point of the lower melting point component to a temperature which is the exact melting point of the solid solution, or crystal alloy desired. This will dissolve an amount of the crucible material (higher melting point compenent) equal to the exact amount required to produce a solid solution having the desired composition. A seed is then introduced into the melt and normal crystal pulling is initiated resulting in the growth of a compositionally ungraded crystal having a uniform compositional content throughout its structure. (Author)

Descriptors :   *PATENTS, *SINGLE CRYSTALS, *SOLID SOLUTIONS, *CRYSTAL GROWTH, ALLOYS, CRUCIBLES, CRYSTALS, HIGH RATE, HIGH TEMPERATURE, LOW TEMPERATURE, MATERIALS, MELTING POINT, MELTS, PURITY, TEMPERATURE

Subject Categories : Crystallography

Distribution Statement : APPROVED FOR PUBLIC RELEASE