Accession Number : ADD015011
Title : Methyl Allyl Telluride.
Descriptive Note : Patent, Filed 13 Jul 87, patented 27 Aug 91,
Corporate Author : DEPARTMENT OF THE NAVY WASHINGTON DC
Personal Author(s) : Higa, Kelvin T ; Harris, Daniel C
Report Date : 27 Aug 1991
Pagination or Media Count : 3
Abstract : A new, unsymmetric allyl-(alkyl) telluride compound has been synthesized and found to be useful as a tellurium source compound in the Metal Organic Chemical Vapor Deposition film growth process. According to the present invention, the new unsymmetric allyl-(alkyl) telluride compound methyl allyl telluride and other unsymmetrical allyl-(alkyl) telluride compounds are prepared by adding an allyl Grignard to a tellurium/tetrahydrofuran slurry and subsequent reaction with an alkyl halide under an inert atmosphere and at temperatures low enough to prevent uncontrolled exothermic reaction. The unsymmetric allyl-(alkyl) telluride product is easily isolated by filtration followed by vacuum distillation. An object of this invention is the new compound allyl methyl telluride.
Descriptors : *TELLURIDES, SYNTHESIS(CHEMISTRY), VAPOR DEPOSITION, ORGANIC COMPOUNDS
Subject Categories : Inorganic Chemistry
Distribution Statement : APPROVED FOR PUBLIC RELEASE